【作者】 房国丽； 张刚； 江涌； 陆有军；

【Author】 Fang Guoli1,~*,Zhang Gang2,Jiang Yong1,Lu Youjun1 1.North University for Ethnics,College of Materials Science and Engineering, Ningxia,Yinchuan,750021; 2.Ningxia University,Academic Journal Center of Ningxia University, Ningxia,Yinchuan,750021

【机构】 北方民族大学材料科学与工程学院； 宁夏大学学术期刊中心；

【摘要】 采用电解腐蚀的方法可控合成了金属Bi纳米粉,所得样品在空气中加热氧化得到Bi2O3纳米晶。通过XRD和SEM的分析表明:一定条件下,pH=12时,所得Bi纳米粉的微观形貌较pH=8时更为均一、尺寸相对较小;氧化温度是影响产物中Bi2O3纳米晶成分和结构的重要因素。更多还原

【Abstract】 Bi nanoparticles have been controlled synthesized via electrolytic corrosion of metal Bi. When the products are thermal retreated in air atmosphere,Bi2O3 nanostructures can be successfully synthesized.The structures,compositions and micro-morphology are characterized by XRD and SEM.The results show that the morphology of the obtained Bi nanoparticles at pH=12 is more uniform than it at pH=8 under the same conditions,and the size is also smaller.One of the important effects on the compositions and microstiuctures of the prepared Bi203 nanocrystals is the oxidized temperature.更多还原