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离子液体[Bmim]BF4中氧化铟的制备研究
Preparation study of indium oxide in ionic liquid
【Author】 XUE Hong WU Qing-hai CHEN Feng LAN Yan-yong TONG Zhang-fa (College of Chemistry and Chemical Engineering,Guangxi University,Nanning 530004,China)
【机构】 广西大学化学化工学院;
【摘要】 室温离子液体作为一种新型的性能优异的绿色环保有机溶剂,在无机材料合成中的应用引起关注.采用微波辅助法和固相研磨法在离子液体[BMIM]BF4 中制备氧化铟,通过差热分析确定了微波法制备的前驱体组成为 In6O10(OH)4,研究了不同制备方法对得到的氧化铟 Zeta 电位的影响.
【Abstract】 As a new type of green environment-friendly solvent,room temperature ionic liquids (RTILs) have been attractive for its abroad applications in the synthesis of the inorganic materials.In this paper,we prepare Indium oxide in the ionic liquid of [BMIM]BF4 through microwave assistant and solid phase grinding respectively,ascertion that the component of the precursor is In6O10(OH)4 by analyzing the DSC figure of the precursor perpared by microwave assistant, then tested Zeta potential of the Indium oxide to discuss the effect of the Zeta potential by different way of preparation.
【Key words】 room temperature ionic liquids; indium oxide; preparation; DSC; Zeta potential;
- 【会议录名称】 第六届中国功能材料及其应用学术会议论文集(10)
- 【会议名称】第六届中国功能材料及其应用学术会议
- 【会议时间】2007-11
- 【会议地点】中国湖北武汉
- 【分类号】O614
- 【主办单位】重庆仪器材料研究所、中国仪器仪表学会仪表材料分会、国家仪表功能材料工程技术研究中心