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阴离子模板法棒状氧化铝制备及性能研究
Synthesis and properties study of alumina nanorods templated by anionic surfactant
【Author】 WANG Jing ZHANG Wen-bo ZHANG Bo XU Xiu-lin (College of Material Science and Engineering,Dalian Jiaotong University,Dalian 116028,China)
【机构】 大连交通大学材料科学与工程学院;
【摘要】 以硝酸铝为原料,利用十六烷基三甲基溴化胺(CTAB)为模板剂,通过水热合成技术制备了棒状氧化铝材料.通过 TEM 及 SEM 分析表明,水合氧化铝产物呈长板片形结构,长径比在1:10左右;经500℃煅烧获得的γ-Al2O3呈棒状,在棒表面有纳米孔洞存在;经1200℃煅烧获得的α-Al2O3则呈现致密的晶粒串烧在一起的棒状结构,但棒的直径不呈等径状态.
【Abstract】 Alumina nanorods were synthesized by hydrothermal technique with Al(NO3)3 as raw material and CTAB as template.TEM and SEM results showed that the structure of hydro-alumina was feature film.The ratio of its length and width was 1:10 or so.The structure of γ-Al2O3 (sintered at 500℃) was rob,and there were nano-holes on the rods.The structure of α-Al2O3 (sintered at 1200℃) was dense powder rod,and its diameter was unlikeness.
- 【会议录名称】 第六届中国功能材料及其应用学术会议论文集(6)
- 【会议名称】第六届中国功能材料及其应用学术会议
- 【会议时间】2007-11
- 【会议地点】中国湖北武汉
- 【分类号】TB383.1
- 【主办单位】重庆仪器材料研究所、中国仪器仪表学会仪表材料分会、国家仪表功能材料工程技术研究中心