节点文献
仙人掌状SnO2/ZnO纳米复合材料的制备及其对NO2的高灵敏快速检测
Synthesis of Cactus-Lke SnO2/ZnO Nanocrystals and Its Highly Sensitive and Rapid Detection of NO2
【摘要】 为了解决纯SnO2基气体传感器对NO2灵敏度低、响应时间长的难题,本文采用水热法制备仙人掌状SnO2/ZnO纳米复合材料,研究了不同配比对SnO2/ZnO复合材料结构形貌与气敏性能的影响。研究结果表明:在水热反应温度180℃、时间6 h,煅烧温度500℃,时间3 h的条件下,SnO2/ZnO配比为35∶1时制得仙人掌状SnO2/ZnO纳米复合材料。NO2气敏特性结果显示,在工作温度300℃条件下,其对10 ppm NO2的响应值可达587.503,响应和恢复时间分别为5 s和39 s,较纯SnO2响应值提升了3.2倍,响应时间缩短了32 s。
【Abstract】 Pure SnO2-based gas sensors are low in sensitivity to NO2 and long in response time.In this study, the hydrothermal method was used to synthesize cactus-like SnO2/ZnO nanocomposites, the impacts of different ratios on their morphological structure and gas sensing performance were investigated.The results show that the cactus-like SnO2/ZnO nanocomposite was obtained under the conditions of the water-thermal reaction temperature of 180 °C for 6 hours, the calcination temperature of 500 °C for 3 hours, and the SnO2/ZnO ratio of 35:1.The NO2 gas sensing characteristics demonstrate that, at the operating temperature of 300 ℃, its response value to 10 ppm NO2 is 587.503 and its response time is 5 s and recovery time 39 s.Compared to pure SnO2,its response value increases by a factor of 3.2 and its response time reduces by 32 s.
【Key words】 SnO2/ZnO composites; gas sensing sensor; NO2; SnO2 nanoflowers;
- 【文献出处】 西安工业大学学报 ,Journal of Xi’an Technological University , 编辑部邮箱 ,2025年01期
- 【分类号】TP212;X831
- 【下载频次】81