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结合剂比例和cBN粒度配比对PcBN复合材料微观结构和性能的影响
Effects of the ratio of binder and the ratio of cBN particle size on the microstructure and properties of PcBN composites
【摘要】 在高温高压条件下制备了聚晶立方氮化硼(PcBN)复合材料。采用X射线衍射(XRD)、扫描电子显微镜(SEM)、能谱仪(EDS)等研究了结合剂配比和立方氮化硼(cBN)粒度对PcBN复合材料的成分、微观结构、显微硬度和磨耗比的影响。实验结果表明:在压力5.5 GPa,温度1 400℃,保温10 min的烧结条件下,当V(TiN0.3)∶V(AlN)=70∶30时,PcBN复合材料性能较为优异,硬度最高达到22.7 GPa,磨耗比达到149.2;当PcBN复合材料中cBN粒度组合为V(0.5~1μm)∶V(2~5μm)∶V(5~10μm)=3∶5∶2时,颗粒之间的堆积密度达到最高,性能也达到最优。
【Abstract】 Polycrystalline cubic boron nitride composites were prepared under high-temperature and high-pressure conditions. The effects of bonding agent ratio and cBN particle size on the composition, microstructure, microhardness, and abrasive ratios of the PcBN composites were investigated using X-ray diffraction(XRD), field scanning electron microscopy(SEM), and energy dispersive spectroscopy(EDS). The experimental results showed that the PcBN composites performed better under sintering conditions of 5.5 GPa, 1 400 ℃, and a 10-minute holding time, achieving a hardness of up to 22.7 GPa and an abrasion ratio of 149.2 at V(TiN0.3)∶V(AlN)=70∶30. Moreover, when the particle size combination of cBN in PcBN composites is(0.5~1) μm:(2~5) μm:(5~10) μm = 3:5:2, the packing density between particles reaches its peak, resulting in optimal performance.
【Key words】 PcBN composite; high pressure and high temperature(HPHT); binder; particle size;
- 【文献出处】 金刚石与磨料磨具工程 ,Diamond & Abrasives Engineering , 编辑部邮箱 ,2024年02期
- 【分类号】TB332
- 【下载频次】11