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超高W含量NiW中/重合金热加工行为研究
Hot Workability of NiW Medium/Heavy Alloys with Ultra-high W Content
【摘要】 采用Gleeble-1500D研究了Ni-42W-10Co-1Mo(质量分数,%)中/重合金(MHA)在1150~1300℃和应变速率0.001~1 s-1下流变行为和微观组织演化规律。结果表明,该合金初始组织由面心立方基体和初生σ相构成。流变应力对变形温度和应变速率敏感,在较高应变速率1s-1下,应力-应变曲线呈现出典型的动态回复软化特征,而在较低应变速率0.1~0.001 s-1下变形应力-应变曲线呈现出典型动态再结晶软化特征。基于应力-应变曲线建立了Arrhenius本构方程,并计算得到Ni-42W-10Co-1Mo合金热变形激活能为446.2 kJ/mol。基于动态材料模型构建该合金热加工图,发现在1300℃高应变速率下存在失稳区。通过微观组织分析,揭示其动态再结晶机制主要为不连续动态再结晶,σ相促进动态再结晶优先在其周围形核。最终优化获得了Ni-42W-10Co-1Mo合金最佳的热加工窗口:1250~1300℃,应变速率0.1~0.01 s-1。
【Abstract】 The flow behavior and microstructural evolution of a high-density Ni-42W-10Co-1Mo(wt%) alloy were investigated at 1150-1300 ℃ under strain rates of 0.001-1 s-1 using a Gleeble-1500D. The results show that the initial microstructure is composed of face-centered cubic matrix and σ phase. The flow stress is sensitive to the deformation temperature and strain rate, and the stress-strain curve shows typical dynamic revertive softening characteristics when deformed at 1 s-1, while typical dynamic recrystallization softening characteristics are observed when deformed at 0.1-0.001 s-1. The Arrhenius equation was established based on the stress-strain curves, and the hot deformation activation energy of the Ni-42W-10Co-1Mo alloy was calculated to be 446.2 kJ/mol. The thermal processing map was constructed based on the dynamic material model to evaluate the thermal processing performance, and the instable zone was located at 1300 ℃under high strain rate. The deformation microstructural evolution reveals that the dynamic recrystallization mechanism is discontinuous dynamic recrystallization, which preferentially nucleates around the σ phase. Finally, the optimized hot working window for Ni-42W-10Co-1Mo alloy was obtained at 1250-1300 ℃ under strain rate of 0.1-0.01 s-1.
【Key words】 MHA; nickel-based alloy; thermal processing; constitutive relationship;
- 【文献出处】 稀有金属材料与工程 ,Rare Metal Materials and Engineering , 编辑部邮箱 ,2024年05期
- 【分类号】TG139
- 【下载频次】54