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高效液相色谱法测定卷烟滤嘴爆珠中8种着色剂

Determination of 8 Synthetic Colorant in Cigarette Filter Rod Capsules by High Performance Liquid Chromatography

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【作者】 顾健龙; 孟红明; 蔡洁云; 唐纲岭; 李中皓; 刘珊珊; 邓惠敏; 马静; 杨兵;

【Author】 Gu Jianlong;Meng Hongming;Cai Jieyun;Tang Gangling;Li Zhonghao;Liu Shanshan;Deng Huimin;Ma Jing;Yang Bing;Yunnan Tobacco Quality Inspection & Supervision Station;National Tobacco Quality Supervision and Inspection Center;

【通讯作者】 孟红明;

【机构】 云南省烟草质量监督检测站; 国家烟草质量监督检验中心;

【摘要】 为深入研究卷烟滤嘴爆珠中着色剂使用情况,建立测定卷烟滤嘴爆珠中柠檬黄、苋菜红、胭脂红、日落黄、诱惑红、酸性红、亮蓝、赤藓红8种着色剂的高效液相色谱法(HPLC),并对市场27种卷烟滤嘴爆珠实际样品进行了着色剂检测分析。建立的方法简单快速,8种着色剂的检出限为0.02~0.07 mg/kg,定量限为0.05~0.20mg/kg,具有较好线性(R~2>0.99)。经检测,酸性红和赤藓红均未检出,其他着色剂检测率在6%~71%之间,检出含量均未超过GB 2760-2014《食品安全国家标准》规定的最大使用量,不存在安全风险。

【Abstract】 In order to further study the use of colorants in cigarette filter beads, the establishment of determination of 8 colorants in cigarette filter beads: lemon yellow, amaranth, carmine, sunset yellow, allure red, acid red, brilliant blue, and erythrosine High Performance Liquid Chromatography(HPLC), and the actual samples of 27 kinds of cigarette filter beads on the market were tested and analyzed for colorants. The established method is simple and fast. The detection limits of the eight colorants are 0.02 mg/kg ~0.07 mg/kg, and the quantification limits are 0.05 ~0.20 mg/kg, with good linearity(R~2>0.99). After testing, neither acid red nor erythrosin was detected, and the detection rate of other colorants was between 6% and 71%, and the detected content did not exceed the maximum use amount specified in GB 2760-2014 "National Food Safety Standard". There is no security risk.

【基金】 中国烟草总公司云南省公司科技计划重点项目卷烟爆珠安全卫生指标检测方法的建立及评价研究(2018530000241032)
  • 【文献出处】 云南化工 ,Yunnan Chemical Technology , 编辑部邮箱 ,2021年01期
  • 【分类号】O657.72;TS452
  • 【下载频次】56
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