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微切变-助剂互作技术辅助提取柑橘皮果胶的工艺研究

Extraction of pectin from citrus peel using press-shear assisted interaction technology

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【作者】 吴菲菲李化强赵良忠徐永平李淑英

【Author】 WU Fei-Fei;LI Hua-Qiang;ZHAO Liang-Zhong;XU Yong-Ping;LI Shu-Ying;College of Food and Chemistry Engineering,Shaoyang University;Hunan Provincial Engineering and Technology Research Center for Fruit and Vegetable Clean Processing;School of Life Science and Biotechnology,Dalian University of Technology;Postdoctoral Research Stations of Dalian SEM Bio-Engineering Technology Co.,Ltd.;

【机构】 邵阳学院食品与化学工程学院湖南省果蔬清洁加工工程技术研究中心大连理工大学生命科学与生物技术学院大连赛姆生物工程技术有限公司博士后科研工作站

【摘要】 目的建立并优化微切变-助剂互作技术提取橘皮果胶的工艺方法。方法采用固态氯化钠为助剂,雪峰蜜橘为主要原料,以果胶的提取率为评价指标,采用单因素和正交实验探索果胶的最优提取工艺,包括Na Cl助剂量、浸提时间、料液比、提取液pH 4个单因素。结果最优工艺条件为:助剂添加量2.5%(m:m)、浸提时间80 min、料液比1:20(m:V,g:mL)、提取液pH为2,此条件下果胶提取率为23.16%,比对照组提高了48.18%,且提取总时长由242 min缩短到102 min。结论以氯化钠为助剂的微切变-助剂互作技术高效省时、安全可靠,为柑橘副产物的高附加值综合利用提供了理论参考。

【Abstract】 Objective To establish and optimize the extraction conditions of pectin from citrus peel using press-shear assisted interaction(PAI) technology. Methods Solid sodium chloride was adopted as additive, Xuefeng tangerine was used as the main raw material, and the yield of pectin was used as the evaluating index. The optimum extraction parameters of pectin from citrus peel were investigated using single-factor test and orthogonal test, which included 4 single factors of the dosage of sodium chloride, extraction time, solid-liquid ratio and extraction solvent pH. Results The optimum technological conditions were as follows: the dosage of sodium chloride was 2.5%(m:m), extraction time was 80 min, solid-liquid ratio was 1:20(m:V, g:mL) and extraction solvent pH was 2, and the highest yield of pectin was up to 23.16%. Under the optimum conditions, the yield of pectin was higher than control group of 48.18%, and the extraction total time was shortened from 242 min to 102 min. Conclusion With the aid of sodium chloride as additive, the PAI technology is efficient, time-saving, safe and reliable, which provides a theoretical reference for the high value-added use of citrus by-products.

【基金】 国家科技部863计划项目(2013AA102805-03);湖南省果蔬清洁加工工程技术研究中心项目(2015TP2022);湖南省自科基金青年项目(2017JJ3284);湖南省教育厅优秀青年项目(17B241);湖南省教育厅一般项目(14C1022,17C1433)~~
  • 【文献出处】 食品安全质量检测学报 ,Journal of Food Safety & Quality , 编辑部邮箱 ,2017年07期
  • 【分类号】TS209
  • 【被引频次】3
  • 【下载频次】205
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