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固相微萃取-气质联用分析柿子甜酒中的香气成分
Analysis of Aroma Constituents in Persimmon Sweet Wine by Solid-phase Micro-extraction and GC-MS
【摘要】 采用固相微萃取法提取柿子甜酒中的香气成分,用气相色谱-质谱仪进行测定,结合计算机检索技术对分离化合物进行分离鉴定,并应用色谱峰面积归一法测定各成分的相对含量。在柿子甜酒中共定性出32中挥发性成分,其中主要包括脂类、醇类、有机酸类、醛类和少量烷烃。结果表明,辛酸乙酯、苯乙醇、癸酸乙酯、邻苯二甲酸二甲酯、2,3-丁二醇等含量相对较高,可能是柿子甜酒香气形成的主要的成分。
【Abstract】 The flavoring compositions were extracted from persimmon sweet wine by solvent extraction and then analyzed by GC/MS.Their relative contents were determined by peak area normalization method.32 volatile compounds were separated and identified,including lipid,alcohols,organic acids,aldehyde and a small amount of paraffin.The detection results showed that ethyl caprylate,phenylethyl alcohol,decanoic acid,ethyl ester,dimethyl phthalate,2,3-butanediol had relatively higher contents than the others,probably being the main flavoring compositions for persimmon sweet wine.
【Key words】 Persimmon sweet wine; solid-phase micro-extraction; GC-MS; the flavoring compositions;
- 【文献出处】 现代食品科技 ,Modern Food Science and Technology , 编辑部邮箱 ,2013年06期
- 【分类号】TS261.7;O657.63
- 【被引频次】9
- 【下载频次】283