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利用毛细管X光透镜共聚焦微束X射线荧光技术对单根头发中元素空间分布进行无损扫描分析

Application of Confocal Micro-Beam X-Ray Fluorescence in Nondestructive Scanning Analysis of the Distribution of Elements in a Single Hair

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【作者】 刘鹤贺刘志国孙天希彭松赵为刚孙蔚渊李玉德林晓燕赵广翠罗萍丁训良

【Author】 LIU He-he;LIU Zhi-guo;SUN Tian-xi;PENG Song;ZHAO Wei-gang;SUN Wei-yuan;LI Yu-de;LIN Xiao-yan;ZHAO Guang-cui;LUO Ping;DING Xun-liang;The Key Laboratory of Beam Technology and Material Modification of the Ministry of Education,Beijing Normal University, College of Nuclear Science and Technology,and Beijing Radiation Center;

【机构】 北京师范大学射线束技术与材料改性教育部重点实验室,核科学与技术学院,北京市辐射中心

【摘要】 头发中的元素与人的饮食和健康状况有关,对头发中元素的分析,不仅可用于刑事物证鉴别,还可为疾病的预防和治疗提供依据,因此,如何检测头发中元素分布等信息倍受人们关注。本文利用基于毛细管X光透镜和实验室普通X射线光源的共聚焦微束X射线荧光技术对单根头进行了无损扫描分析,分析了单根头发中元素的空间分布。在该毛细管X光透镜共聚焦微束X射线荧光技术中,毛细管X光会聚透镜的出口焦斑和毛细管X光平行束透镜的入口焦斑处在共聚焦状态,从而形成共聚焦微元,探测器只能探测到来自该共聚焦微元中的X射线信号,降低了背底信号对X射线荧光谱的影响,从而有利于提高该共聚焦X射线荧光技术的分析精度。该共聚焦技术中采用了具有高功率密度增益的毛细管X光会聚透镜,降低了该共聚焦X射线荧光技术对X射线光源功率的要求,从而保证了该共聚焦技术可以采用实验室普通X射线光源,降低了实验成本。实验表明,毛细管X光透镜共聚焦微束X射线荧光技术在单根头发元素分布检测中具有应用价值。

【Abstract】 The confocal micro X-ray fluorescence(XRF)based on polycapillary X-ray lens and conventional X-ray source was used to carry out the scanning analysis of the distribution of the elements in a single hair.The elemental distribution in the single hair was obtained.In the confocal micro XRF technology,the output focal spot of the polycapillary focusing X-ray lens and the input focal spot of the polycapillary parallel X-ray lens were adjusted confocally.The detector could only detect the X-rays from the overlapping foci.This confocal structure decreased the effects of the background on the X-ray spectra,and was accordingly helpful for improving the accuracy of this XRF technology.A polycapillary focusing X-ray lens with a high gain in power density was used to decrease the requirement of power of the X-ray source used in this confocal technology,and made it possible to perform such confocal micro XRF analysis by using the conventional X-ray source with low cost.Experimental results indicated that the confocal micro X-ray fluorescence based on polycapillary X-ray lens had potential applications in analyzing the elemental distribution of individual hairs.

【基金】 国家自然科学基金项目(11075017);北京市优秀人才培养项目(2010C009012000005)资助
  • 【文献出处】 光谱学与光谱分析 ,Spectroscopy and Spectral Analysis , 编辑部邮箱 ,2013年11期
  • 【分类号】O434.1
  • 【被引频次】3
  • 【下载频次】259
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