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水热法制备片状氧化铝纳米粉体
Preparation of Plate-Like Alumina Nanometer Powder by Hydrothermal Method
【摘要】 在碳酸氢铵和PEG2000混合溶液中,加入硫酸铝铵和PEG400的混合溶液得到白色沉淀,将白色沉淀物与正丁醇共沸后,在900℃煅烧1h,得到γ-Al2O3粉体,粉体粒径约为20nm;在1200℃煅烧1h,得到片状α-Al2O3粉体,粉体粒径约为60nm。
【Abstract】 When the solution with aluminium ammonium sulfate and PEG400 was mixed with the solution content of ammonium hydrogen carbonate and PEG2000,the white precipitation was obtained.Then the precipitation was azeotropic distillation.The γ-Al2O3 powder was obtained at 900 ℃ for 1 h,with size about 20 nm.The plate-like α-Al2O3 powder was obtained at 1 200 ℃ for 1 h,with size about 60 nm.
- 【文献出处】 陶瓷 ,Ceramics , 编辑部邮箱 ,2012年11期
- 【分类号】TB383.1
- 【被引频次】9
- 【下载频次】345