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土壤中酞酸酯类化合物监测方法的质量控制研究

The Quality Control in the Monitoring Methodsfor Phthalate Esters in Soil

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【作者】 邓慕夏新王伟马芳池靖多克辛

【Author】 DENG Mu1 ,XIA Xin2 ,WANG Wei3 ,MA Fang1 ,CHI Jing2 ,DUO Ke-xin3 ( 1. Beijing Science and Technology University,Beijing 100083,China; 2. China National Environmental Moni- toring Center,Beijing 100012,China; 3. Henan Environmental Monitoring Center,Zhengzhou,Henan 450004, China )

【机构】 北京科技大学中国环境监测总站河南省环境监测中心

【摘要】 从监测结果控制的角度对近10年的土壤中PAEs监测方法进行了探讨,重点比较了索氏萃取柱净化GC/MS、微波萃取柱净化GC、加速溶剂萃取柱净化GC/MS和加速溶剂萃取GPCGC/MS方法的检出限、精密度和准确度。旨在为中国土壤监测方法的建立提供基础支撑,为开展质量控制工作提供评价依据。

【Abstract】 The monitoring methods for phthalate esters( PAEs) in soil in recent 10 years was discussed from monitoring results control. The detection limit,precision and accuracy between the four monitoring methods including soxhlet extraction-column purification GC/MS,microwave extraction-column purification GC,accelerated solvent extraction-column purification GC/MS and accelerated solvent extraction GPC GC/MS method were compared in this study. This paper aimed to provide basic support for the establishment of soil monitoring method,and offer evaluating basis for the conduct of quality control.

【关键词】 土壤酞酸酯监测方法质量控制
【Key words】 soilphthalate estersmonitoring methodquality control
【基金】 环保公益性行业科研专项项目(200809140)
  • 【文献出处】 环境监控与预警 ,Environmental Monitoring and Forewarning , 编辑部邮箱 ,2012年01期
  • 【分类号】X833
  • 【被引频次】4
  • 【下载频次】147
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