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流动注射-氢化物发生-原子荧光光谱法测定牛奶中的铅
Determination of Lead in Milchigs by HG-AFS with Flow Injection
【摘要】 建立了流动注射-氢化物发生-原子荧光光谱法测定奶制品中铅含量的分析方法,对仪器条件和反应条件进行了选择、优化。方法的检出限为0.30μg/L,相对标准偏差小于4.7%,回收率为90.0%—114.5%,符合食品中痕量元素的分析要求。
【Abstract】 The analytical method for the determination of the content of lead in milchigs was established by flow injection-hydride generation-atomic fluorescence spectrometry(HG-AFS).The conditions of instrument and reaction were choosed and optimized.The detection limit of the method was 0.30μg/L and the RSD was less than 4.7%,and the recoveries were in the range of 90.0%—114.5%,and that met the analytical requirements of trace elements in foods.
【关键词】 原子荧光光谱法;
氢化物发生;
食品;
铅;
【Key words】 Atom Fluorescence Spectrometry; Hydride Generation; Foods; Lead;
【Key words】 Atom Fluorescence Spectrometry; Hydride Generation; Foods; Lead;
【基金】 安康学院科研资金资助项目(2010AKXYDXS08)
- 【文献出处】 光谱实验室 ,Chinese Journal of Spectroscopy Laboratory , 编辑部邮箱 ,2012年02期
- 【分类号】TS252.7;O657.31
- 【被引频次】1
- 【下载频次】91