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溶液法制备CeO2纳米材料

Synthesis of CeO2 Nanoparticles by Solution Method

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【作者】 张朝霞张国庆汪丽娜邵敏

【Author】 ZHANG Zhaoxia,ZHANG Guoqing,WANG Lina,SHAO Min (Key Laboratory of Advanced Textile Materials and Manufacturing Technology of Ministry of Education, Zhejiang Sci-Tech University,Hangzhou 310018)

【机构】 浙江理工大学先进纺织材料与制备技术教育部重点实验室

【摘要】 以硝酸铈为铈源,聚乙烯吡咯烷酮为表面活性剂,在碱性水相条件下制备CeO2纳米微晶。用XRD、SEM和TEM对产物进行表征,结果显示得到的CeO2纳米微晶具有立方晶型结构,分散性好,直径为10~20nm。此外,用紫外-可见分光光度计对样品的紫外吸收性质进行了考察。

【Abstract】 The CeO2 crystals were synthesized by a solution method using Ce(NO3)3·6H2O and polyvinylpyrrolidone(PVP) as precursors.X-ray powder diffraction,field emission scanning electron microscopy and transition electron microscopy were used to characterize the obtained samples.The results showed that cubic crystalline CeO2 nanoparticles of 10~20nm in size and with good monodispersity were obtained using this method.In addition,the UV absorption properties of the CeO2 nanoparticles were studied by UV-Vis spectroscopy.

【关键词】 纳米CeO2紫外吸收合成
【Key words】 CeO2UV absorptionsynthesis
【基金】 浙江省自然科学基金(Y4090167);浙江理工大学科研启动基金
  • 【文献出处】 材料导报 ,Materials Review , 编辑部邮箱 ,2011年S2期
  • 【分类号】TB383.1
  • 【被引频次】2
  • 【下载频次】152
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