【摘要】 以苯甲醇和三氯化磷为原料,通过三步反应合成了二苄基磷酸酯,总收率67.4%,其结构经IR表征。以三乙胺为缚酸剂,四氯化碳为前两步反应共同的溶剂,省略了第一步反应结束后的溶剂分离操作。更多还原

【Abstract】 Dibenzyl phosphate in overall yield of 67.4% was synthesized by a three-step reaction from benzalcohol with phosphorus trichloride.The structure was characterized by IR.Triethylamine was used as the acid binding agent.Carbon tetrachloride was used as the solvent in the first and second reaction,so separation of solvent was simplifed.更多还原