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AZ31镁合金沉积Mg-Cu-Y非晶薄膜的结构与性能
Structure and properties of Mg-Cu-Y amorphous film deposited on AZ31 alloy
【摘要】 采用非平衡磁控溅射方法在AZ31镁合金表面沉积Mg-Cu-Y薄膜,以纯铜和Mg65Cu25Y10合金作为溅射靶材,选则Mg65Cu25Y10单靶、Mg65Cu25Y10靶和铜靶双靶两种方式分别进行溅射沉积。利用XRD、AFM、SEM分析了膜层结构与表面形貌,纳米压痕法、球盘式摩擦磨损测试研究了膜层的硬度和耐磨性。结果表明,Mg65Cu25Y10单靶溅射得到的薄膜为完全非晶态结构,而双靶共溅获得的膜层中出现含有铜的晶态组织。随着膜层中Cu含量的增加,纳米硬度较非晶态膜层有所降低,但同时耐磨性提高。两类不同结构薄膜相比较,Mg65Cu25Y10单靶溅射沉积的非晶膜层硬度最高,达到12GPa。用磨损量评价了基体与膜层的耐磨性,包含Cu结晶相的双靶共溅薄膜具有较好的耐磨性能。
【Abstract】 Mg-Cu-Y films were deposited on AZ31 alloy by unbalanced magnetron sputtering.The targets made of pure copper and Mg65Cu25Y10 alloy were adopted.The depositions were carried out by two different modes,that is,deposition by using Mg65Cu25Y10 alloy target alone and co-deposition with Mg65Cu25Y10 alloy target and copper target.The phases of the deposited films were analyzed by glancing incidence X-Ray diffraction(GXRD).The morphology of the films and the wear traces were observed by atom force microscope(AFM) and scanning electronic microscopy(SEM),respectively.The hardness of the films was measured by nano-indentation tests.The friction tests were conducted on a ball-disk friction tester.The results show that the structure of the film deposited by Mg65Cu25Y10 is amorphous and no crystalline phase is found.For the films deposited by co-depositition,crystalline copper is detected.The film deposited by Mg65Cu25Y10 exhibits the maximum hardness of 12GPa.The film containing crystalline copper phase deposited by co-depositition shows the better wear resistance.
【Key words】 Mg-Cu-Y films; co-sputtering deposition; hardness; friction and wear;
- 【文献出处】 材料热处理学报 ,Transactions of Materials and Heat Treatment , 编辑部邮箱 ,2009年02期
- 【分类号】TG174.44
- 【被引频次】4
- 【下载频次】221