【摘要】 采用单酯化法合成三氯蔗糖,并建立了气相色谱-质谱(GC/MS)检测合成过程中各重要组分的方法。采用HP-5毛细管气相色谱柱(30 m×0.25 mm×0.25μm),以电子轰击为电离方式,选取最佳实验条件对蔗糖、蔗糖-6-乙酯、三氯蔗糖进行硅烷化衍生,并对其进行定性、定量检测。该检测方法用于监测单酯化法合成三氯蔗糖的工艺过程,取得了理想效果。更多还原

【Abstract】 Sucralose was synthesized by monoesterification method. A method was established of gas chromatography-mass spectrometry for determination of sucrose,sucrose-6-acetate and sucralose.The operating conditions were HP-5 column(30 m×0.25 mm×0.25 μm) and EI.It is used for monitoring and improving the steps of synthesis sucralose.更多还原