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超大挤压变形对钛合金增强镁基复合材料显微组织的影响

Effect of Ultra-Deformation on the Microstructures of Titanium Alloy Reinforced Magnesium Matrix Composites

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【作者】 郗雨林柴东朗王耀玮

【Author】 Xi Yulin1,2, Chai Donglang2, Wang Yaowei2 (1. Luoyang Ship Material Research Institute, Luoyang 471039, China) (2. Xi’an Jiaotong University, Xi’an 710049, China)

【机构】 洛阳船舶材料研究所西安交通大学西安交通大学 河南洛阳471039 西安交通大学陕西西安710049

【摘要】 采用粉末冶金法制备了钛合金(Ti-6Al-4V)(质量分数,下同)颗粒增强MB15镁基复合材料,经225:1的超大比热挤变形后,借助光学显微镜(OM)、扫描电镜(SEM)和透射电镜(TEM)对其显微组织进行了研究。结果表明:钛合金颗粒沿挤压方向因塑性变形而被拉长,其增强效果得到提高;超大比热挤变形能够显著细化基体晶粒,并提高复合材料的组织均匀性;此外,原镁粉表面的氧化膜经超大比变形后得到了有效的碎化和分散,具有一定的弥散强化效果,因此可充当粉末冶金制备镁基复合材料的辅助增强相。

【Abstract】 Magnesium matrix composite reinforced by titanium alloy (Ti-6Al-4V) particulate was fabricated by powder metallurgy route. The samples of composite were hot-extruded with an ultra-deformation ratio of 225:1. The microstructures of extruded samples were investigated using optical microscopy, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The results showed that the Ti-6Al-4V particulates were apparently elongated along the extrusion direction, thus increased its reinforcing effect on the matrix. The ultra-deformation could markedly decrease the grain sizes of the composite matrix, and greatly improve the homogeneity of microstructures when compared with a lower ratio of extrusion deformation; in addition, the oxide layers on the surface of original Mg particles were effectively broken and dispersed randomly in the vicinity of Mg-Mg interfaces. It produced an oxidedispersion-strengthening (ODS) effect, further reinforced the matrix as a kind of secondary reinforcement.

【基金】 国家自然科学基金(50471032);科技部重大项目前期专项(02061005)资助
  • 【文献出处】 稀有金属材料与工程 ,Rare Metal Materials and Engineering , 编辑部邮箱 ,2007年05期
  • 【分类号】TB331;TG113.12
  • 【被引频次】2
  • 【下载频次】276
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