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微波强化提取杜仲叶中绿原酸的工艺研究

Study on extracting process of caffetannic acid from folium cortex eucommiae via microwave

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【作者】 李剑敏卫兵兵陈志红

【Author】 LI Jian-min~1,WEI Bing-bing~2,CHEN Zhi-hong~1(1.School of Environmental Science and Engineering,Chang’an University,Xi’an 710054,China;2.Hualu Engineering and Technology Co.,Ltd,Xi’an 710054,China)

【机构】 长安大学环境科学与工程学院华陆工程科技有限公司长安大学环境科学与工程学院 陕西西安710054陕西西安710054

【摘要】 对杜仲叶中的绿原酸提取工艺进行了研究,结果表明,采用微波破壁可以明显的提高杜仲叶绿原酸的提取率。优化的工艺条件为以水为溶剂,加水量在20%,微波破壁3次,每次30 s,pH为5.8时,绿原酸具有较高的提取率。微波破壁与传统的水回流法、醇回流法相比较,具有成本低、产物收率高、可显著降低提取液中杂质含量的优点。

【Abstract】 In this paper,the process of extracting caffetannic acid from folium cortex eucommiae was investigated.The results indicated that the yield of caffetannic acid from folium cortex eucommiae have a noticeable improvement with the induction of microwave.Further,the results showed that when choosing water as solvent,the dosage of water is 20%,the cell wall destroyed for three times and each time lasts 30 s,pH value is 5.8,the yield of caffetannic acid would get a higher level.Comparing with the traditional single reflux route of water solute,ethanol or methanol solute,the present methods would decrease the impurities in the products distinctly,and lower the costs obviously.Besides,the present method with high yield.

【关键词】 杜仲绿原酸提取微波
【Key words】 eucommiaecaffetannic acidextractingmicrowave
【基金】 国家“973”项目(G1999403606)
  • 【文献出处】 应用化工 ,Applied Chemical Industry , 编辑部邮箱 ,2006年04期
  • 【分类号】TQ463.25
  • 【被引频次】28
  • 【下载频次】347
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