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热处理对原位自生Mg2Si/Mg-Al基复合材料组织与性能的影响
Influence of solution heat treatment and ageing on microstructure and properties of in-situ Mg2Si/Mg-Al matrix composite
【摘要】 利用金属型铸造制备了原位自生Mg2Si/Mg-Al基复合材料,研究了热处理对该材料组织与性能的影响。结果表明T4处理改变了Mg2Si/Mg-Al基复合材料中Mg2Si的形貌与分布。随着保温时间的延长,棱状枝晶Mg2Si相发生熔断、球化,最终成为尺寸为10-30μm的颗粒;同时β-Mg17Al12相溶入到α-Mg基体中,在随后的时效过程中发生沉淀析出。由于β-Mg17Al12相的溶解,T4处理会降低该材料的硬度,但随后的时效析出可提高其硬度,415℃×12h固溶处理后175℃×16h(T6)时效,硬度可提高14.9%。热处理过程中棱状枝晶Mg2Si相的粒化可用吉布斯-汤姆逊定理解释。
【Abstract】 In-situ Mg2Si/Mg-Al matrix composite was prepared by permanent mold casting.The effects of heat treatment on microstructure and properties of in-situ Mg2Si/Mg-Al matrix composite were investigated.The results show that the morphology and distribution of Mg2Si in the Mg2Si/Mg-Al matrix composite are changed during T4 heat treatment.With increasing holding time,the roughly prismatic dendritic Mg2Si phase tends to be dissolved and broken and spheroidized and finally transformed into particles with size of 10-30μm; at the same time,the β-Mg 17 Al 12 phase is dissolved into the matrix to form supersaturated solid solution of α-Mg,then precipitates during subsequent ageing heat treatment.Due to solution of β-Mg 17 Al 12 phase,the hardness of the composite decreases after T4 treatment,and then increases during subsequent ageing treatment.The hardness is improved by 14.9% after 415℃×12h solution heat treatment and then aging at 175℃ for 16h(T6 treatment).The spheroidization of roughly prismatic dendritic Mg2Si phase during heat treatment can be explained by Gibbs-Thomson’s theorem.
【Key words】 magnesium alloys; in-situ composite; in-situ reaction; heat treatment;
- 【文献出处】 材料热处理学报 ,Transactions of Materials and Heat Treatment , 编辑部邮箱 ,2006年06期
- 【分类号】TB331
- 【被引频次】46
- 【下载频次】484