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多晶粉末样品热膨胀的X射线衍射测量
Thermal Expansion of Multi-crystal Powder Measured by X-ray Diffractometer
【摘要】 利用X射线衍射方法精确测量了2∶17型稀土化合物N d2A lFe15M n的晶胞参数及热膨胀系数并研究了其结构特征.结果表明,室温下,N d2A lFe15M n化合物具有单相的Th2Zn17型菱方结构(空间群为R 3m).对该化合物晶格常数的测量误差可以达到1-0 4,基本上可满足对一般位移型相变测量要求的精度.
【Abstract】 The lattice constants and the thermal expansion coefficient of 2∶17 type rare earth-transition metal compound Nd2AlFe15Mn were obtained by means of X-ray diffraction.The results showed that Nd2AlFe15Mn compound has a rhombohedral Th2Zn17-type structure in room temperature.The errors of lattice constant in this compound were able to achieve 10-4,which basically met the measuring precision in displacive phase transition.
【基金】 国家自然科学基金资助项目(50271022);天津师范大学博士基金资助项目(52R010)
- 【文献出处】 天津师范大学学报(自然科学版) ,Journal of Tianjin Normal University (Natural Science Edition) , 编辑部邮箱 ,2005年04期
- 【分类号】TB44
- 【被引频次】3
- 【下载频次】177