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碳纳米管/镍复合镀层硬度研究

Hardness of Carbon Nanotubes /Nickel Composite Coating Prepared by Electrodeposition

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【作者】 林文松; 周细应; 王思珺; 李轶;

【Author】 LIN Wen-song, ZHOU Xi-ying, WANG Si-jun, LI Tie (Shanghai University of Engineering and Science, Shanghai 200336, China)

【机构】 上海工程技术大学材料工程学院; 上海工程技术大学材料工程学院 上海200336; 上海200336; 上海200336;

【摘要】 在瓦特镀镍溶液中加入碳纳米管,研究球磨处理、搅拌分散形式、分散剂对碳纳米管在镀液中均匀稳定分散的影响,采用恒电流电沉积工艺制备了碳纳米管/镍复合镀层。结果表明:碳纳米管球磨后加入到镀液中,并通过超声分散,可以得到稳定的复合电镀液;碳纳米管与镍能很好地共沉积。当阴极电流密度为2.5A/dm2、镀液温度为45℃、碳纳米管加入量为0.8-1.2g/L时镀层显微硬度达到最大值。

【Abstract】 Carbon nonotubes (CNTs) / Ni bath and CNTs / Ni composite coating were prepared. The homogenous dispersion stability of the bath and the microhardness of CNTs / Ni composite coating were studied. The results indicated that CNTs were stably suspended in nickel bath after ball-mill treatment and supersonic dispersion. The microhardness of the composite coating was increased to 250 HV when current density was 2. 5 A/ dm2, bath temperature was 45℃ and CNTs content in the bath was 0. 8-1. 2 g/L. The SEM image of the coating showed that CNTs were embedded in the matrix uniformly.

【关键词】 电沉积; 复合镀层; 碳纳米管;
【Key words】 electrodepositition; composite coating; carbon nanotube;
【基金】 上海市科委纳米专项基金资助项目(0211nm050)
  • 【文献出处】 机械工程材料 ,Materials For Mechanical Engineering , 编辑部邮箱 ,2005年04期
  • 【分类号】TQ153
  • 【被引频次】17
  • 【下载频次】275
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