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合金化热镀锌IF钢板镀层显微组织的TEM观察

CROSS-SECTIONAL TEM OBSERVATION ON COATING MICROSTRUCTURE OF GALVANNEALED IF STEEL SHEETS

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【作者】 余金山; 张津徐; 吴建生; 刘俊亮; 陈家光;

【Author】 YU Jin-shan~1, ZHANG jin-xu~1, WU Jian-sheng~1, LIU Jun-liang~2, CHEN Jia-guang~2 (1. School of Material Science and Technology, ShangHai JiaoTong University, Shanghai 200030, China; 2. Physical Testing Section of testing Center, Baosteel Groups, Shanghai 201900, China)

【机构】 上海交通大学材料科学与工程学院; 宝钢分析测试中心物理室; 宝钢分析测试中心物理室 上海200030; 上海200030; 上海201900; 上海201900;

【摘要】 介绍了用聚焦离子束方法制备合金化热镀锌IF钢板镀层横截面TEM试样,应用透射电镜对其显微结构进行了观察。结果表明,商用合金化热镀锌IF钢板镀层显微结构由近界面的牙齿状Γ相层和等轴Γ1相及δ相组成,晶粒尺寸为0.5~1μm;δ相电子衍射斑点中存在明显的超点阵斑点。

【Abstract】 The coating microstructure of galvannealed IF steel sheets was studied by TEM. The cross-sectional TEM specimen was prepared using Focused Ion Beam technique which was also introduced briefly. The results show that the coating microstructure of commercial galvannealed IF steel sheets consist of Γ phase which appears front-teeth micrograph adjacent to the Fe-Zn interface and Γ1, δ phase which appear equiaxed crystal micrograph. It also show that the grain size is 0.5~1μm and it exits superlattice reflections in the electron diffraction pattern of δ phase.

【关键词】 合金化热镀锌; 聚焦离子束; 透射电镜;
【Key words】 Galvanneal; FIB; TEM;
【基金】 国家自然科学基金项目(50171040)
  • 【文献出处】 理化检验(物理分册) ,Physical Testing and Chemical Analysis Part A Physical Testing , 编辑部邮箱 ,2004年11期
  • 【分类号】TG174
  • 【被引频次】3
  • 【下载频次】239
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