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细晶钨铜复合材料制备工艺的研究

Study of process of fine-grained W-Cu composites

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【作者】 范景莲刘军严德剑黄伯云

【Author】 Fan Jinglian,Liu Jun,Yan Dejian,Huang Baiyun (State Key Laboratory for Powder Metallargy,Contral South University,Changsha 410083,China)

【机构】 中南大学粉末冶金国家重点实验室中南大学粉末冶金国家重点实验室 长沙410083长沙410083长沙410083

【摘要】 将W 2 0 %Cu混合粉末在行星式高能球磨机中机械合金化 (MA)。经过一定时间球磨后可以得到W晶块尺寸 30nm左右的纳米粉末。测定了粉末晶粒尺寸、粉末的粒度、比表面、松装密度和振实密度等性能。粉末的晶块尺寸用XRD分析得出。研究了MAW 2 0 %Cu粉末烧结后的显微组织。研究表明 ,球磨后粉末在 12 0 0~ 130 0℃下烧结即可达到近全致密 ,相对密度在 99 5 %以上 ,拉伸强度达到 780MPa以上 ,伸长率大于 3 5 % ,钨晶粒尺寸在 1~ 2 μm左右。

【Abstract】 Elemental W-20%Cu powder mixtures were mechanically alloyed in a planetarg high ball milling. After a certain time of high-energy ball milling, nanostructured W-Cu composite powder was obtained where W crystalline size about 30nm. Crystalline sizes of milled powder were analyzed by means of XRD. Meanwhile the powder characterization such as particle size, distribution, apparent density and tap density of MA-ed powder were examined. The green part from the nanostructured powder was then sintered at 1200~1300 ℃ . The relative density of the sample is higher than 99.5%, tensile strength is higher than 780MPa, elongation of the samples higher than 3.5% and tungsten grain is about 1~2μm.

【关键词】 机械合金化钨-铜细晶材料烧结
【Key words】 mechanical alloyingW-Cunanocrystalline powdersintering
【基金】 湖南省科学技术重点基金项目 (0 1JZY2 0 5 7)
  • 【文献出处】 粉末冶金技术 ,Powder Metallurgy Technology , 编辑部邮箱 ,2004年02期
  • 【分类号】TB331
  • 【被引频次】71
  • 【下载频次】554
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