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丹参的毛细管电泳指纹图谱研究
Study on CE fingerprint of Salvia miltiorrhiza
【摘要】 目的 :利用毛细管电泳技术建立丹参中药材的指纹图谱。方法 :采用 5 0 μm× 5 0cm未涂渍毛细管柱 ,2 0mmol/L硼砂溶液作缓冲液 ,运行电压为 15kv ,检测波长为 2 10nm。结果 :建立的指纹图谱中共有 11个共有峰 ,且方法学考察符合规定的标准。结论 :该法准确简便 ,可作为控制丹参药材内在质量的有效手段。
【Abstract】 Objective: To investigate the CE fingerprint of Salvia miltiorrhiza . Methods : Separation was performed on a 50μm×50cm uncoated capillary with 20mmol·L -1 borate solution as CE buffer. The run voltage was 15kV and the UV detection was set at 210nm. Results : Fingerprint consisted of 11 common peaks. The validation of methods meet the requirements for SDA’s technical regulations. Conclusion : The method was accurate and simple for quality control of Salvia miltiorrhiza.
- 【文献出处】 中成药 ,Chinese Traditional Patent Medicine , 编辑部邮箱 ,2003年12期
- 【分类号】R284
- 【被引频次】59
- 【下载频次】480