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纳米金属多层膜与多层纳米线的电化学制备及其表征

Electrochemical Preparation and Characterization of Metal Multilayers and Metal Multilayer Nanowires

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【作者】 迟广俊冯钊永赵瑾姚素薇

【Author】 Chi Guang Jun Feng Zhao Yong Zhao Jin Yao Su Wei(School of Chemical Engineering and Technology,Tianjin University,Tianjin 300072)

【机构】 天津大学化工学院天津大学化工学院 天津300072天津300072天津300072

【摘要】 分别采用单槽法和双槽法电沉积Cu/Co多层膜.研究了两种电沉积方法制备多层膜的工艺条件,利用电化学方法、XRD和SEM对多层膜进行表征,并对Cu/Co多层膜的巨磁阻性能进行了测试.采用电沉积多层膜的方法,以多孔铝阳极氧化膜(AAO)为模板,在纳米孔内沉积Cu/Co多层线,采用TEM对多层纳米线进行了表征.

【Abstract】 Cu/Co multilayers were prepared by single bath technology (SBT) and double bath technology (DBT),respectively.The technological conditions of SBT and DBT were studied.Using electrochemical method ,XRD and SEM,the layer structureof the prepared multilayer was affirmed.The magnetoresistance property of Cu/Comultilayers was measured and the results show that the GMR of Cu/Co multilayersis 7.5%at 2500 Gs.On the base of the preparation of Cu/Co multilayers,Cu/Co multilayer nanowires arrays on porous anodic aluminum oxide templates were fabricated and its structure was characterized by TEM.The micrographs exhibited that the diameter of the Cu/Co multilayer nanowires is about 120 nm and length up to 10 μm.

【基金】 国家自然科学基金(50271046);教育部、天津大学南开大学联合研究院资助项目~
  • 【文献出处】 物理化学学报 ,Acta Physico-chimica Sinica , 编辑部邮箱 ,2003年02期
  • 【分类号】O646
  • 【被引频次】40
  • 【下载频次】485
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