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油菜蜂花粉中脂肪酸的GC-MS分析
Analysis of Fatty Acids in Rape Pollen by GC-MS
【摘要】 以石油醚和乙醚为溶剂 ,采用索氏抽提法提取油菜蜂花粉中的粗脂肪 ,进行甲酯化处理 ,并用GC -MS技术对脂肪酸甲酯进行分离鉴定 ,共鉴定出10种脂肪酸 ;测定其相对含量 ,其中不饱和脂肪酸相对含量高达76.0 % ,多不饱和脂肪酸相对含量为53.2 %。
【Abstract】 The rough fat in rape pollen was abstracted by Soxhlet extraction method with petroleum ether-ethyl ether mixed solvents, then methylated, and the methylated fatty acids were analyzed by GC-MS. Ten fatty acids were identified and their relative contents were determined by normalization method of area. The analyzed results exhibited that the unsaturated fatty acids content reached up to 76.0%, and polyunsaturated acids accounted for 53.2%.
【基金】 中华全国供销合作总社科学技术发展计划资助项目 (2000科研 -9)
- 【文献出处】 分析测试学报 ,Journal of Instrumental Analysis , 编辑部邮箱 ,2003年01期
- 【分类号】O657.63
- 【被引频次】40
- 【下载频次】321