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非水滴定法测定盐酸甜菜碱的含量
Nonaqueous titration for determination of betaine hydrochloride
【摘要】 目的 建立测定盐酸甜菜碱含量的非水滴定法。方法 样品以冰醋酸作溶媒 ,以结晶紫为指示剂 ,用0 1mol·L-1标准高氯酸溶液进行滴定。结果 平均回收率为 99 81% ,RSD为 0 19%。结论 本方法准确、稳定、简便 ,易于推广
【Abstract】 Objective: To establish a nonaqueous titration method for the determination of betaine hydrochloride. Methods: Ice vinegar was used as solvent, and 0.2% viola crystalline used as indicator. Betaine hydrochloride was titrated by 0.1 mol·L -1 perchloric acid solution. Results: The average recovery rate was 99.81%(n=5), and RSD was 0.19%. Conclusion: The method is simple, reliable and accurate.
【关键词】 盐酸甜菜碱;
非水滴定法;
含量测定;
【Key words】 betaine hydrochloride; nonaqueous titrations; quantitative determination;
【Key words】 betaine hydrochloride; nonaqueous titrations; quantitative determination;
- 【文献出处】 泰山医学院学报 ,Journal of Taishan Medical College , 编辑部邮箱 ,2002年04期
- 【分类号】R284
- 【被引频次】31
- 【下载频次】353