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羟基磷灰石合成工艺研究

Study on the technique conditions for the synthesis of hydroxyapatite ceramic powder

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【作者】 童义平; 余木磷; 钟秀兰; 曾翠石令;

【Author】 TONG Yi ping,YU Mu lin,ZHONG Xiu lan,ZENG Cui ling (Department of Bio chemistry,Hanshan Normal College,Chaozhou 521041,China)

【机构】 韩山师范学院化生系; 韩山师范学院化生系 福建潮州521041; 福建潮州521041; 福建潮州521041;

【Abstract】 The technique conditions of synthesis of hydroxyapatite(HAP) powder were studied by Sol Gel and chemical coprecipitation processes.The FTIR was applied to determine the chemical composition of the prepared product.The Ca/P ratio was determined also and compared with stoichimetric ratio of hydroxyapatite.The cross experiment result indicated that the optimum technique condition to gain high purity HAP powder involves Ca/P 1.67 ,pH 8.0,temperature 950℃,reaction time 3.5h when (C 4H 9O) 3PO and Ca(NO 3) 2 were used as starting materials;Ca/P 1.67 ,temperature 37.5℃,pH 9.0 and Ca/P 1.50,temperature 80℃,pH 11.0 when H 3PO 4 and Ca(OH) 2 were used as starting materials;and Ca/P 1.50,temperature 37.5℃,pH 9.0,Ca/P 1.67,temperature 50℃,pH 9.0 and Ca/P 1.67,temperature 70℃,pH 10.0 when (NH 4) 2HPO 4 and Ca(NO 3) 2 were used as starting materials.

  • 【文献出处】 化学研究与应用 ,Chemical Research and Application , 编辑部邮箱 ,2002年01期
  • 【分类号】R914
  • 【被引频次】24
  • 【下载频次】318
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