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薄层扫描法测定小儿解热宁口服液中柴胡皂苷b2的含量
DETERMINATION OF SAIKOSAPONIN b2 IN XIAO′ER JIERENING ORAL LIQUID BY TLC SCANNING
【摘要】 目的 :建立小儿解热宁口服液的含量测定方法。方法 :采用薄层扫描法对小儿解热宁口服液中柴胡皂苷b2 进行定量。结果 :柴胡皂苷b2 在 0 .6~ 2 .8μg范围内与峰面积积分值呈良好的线性关系 ,平均回收率为 97.0 9% ,RSD =1.2 4 % (n =5 )。结论 :本法简便、快速、准确 ,可作为小儿解热宁口服液质量控制的方法。
【Abstract】 Objective:To establish a method for the determination of Xiao′er Jierening oral liquid.Method:Thin layer chromatography scanning was used to determine the contents of saikosaponin b 2 in Xiao′er Jierening oral liquid. Result:The standard curve of saikosaponin b 2 was linear in the range of 0.6~2.8 μg.The average recovery was 97.09%. Conclusion:The method was simple,sensitive and accurate,thus it may be used for quality control of Xiao′er Jierening oral liquid.
【关键词】 小儿解热宁口服液;
柴胡皂苷b2;
薄层扫描法;
【Key words】 Xiao′er Jierening oral liquid; Saikosaponin b 2; Thin layer chromatography scanning;
【Key words】 Xiao′er Jierening oral liquid; Saikosaponin b 2; Thin layer chromatography scanning;
- 【文献出处】 安徽中医学院学报 ,Journal of Anhui Traditional Chinese Medical College , 编辑部邮箱 ,2002年05期
- 【分类号】R286
- 【被引频次】9
- 【下载频次】157