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大豆低聚糖制取与纯化工艺的研究
STUDY ON EXTRACTION AND PURIFICATION TECHNOLOGY OF SOYBEAN OLIGOSACCHRIDE
【摘要】 本文以低温脱脂大豆粕为原料 ,比较了多种溶剂对大豆低聚糖的浸提效果 ,确定较优的浸取条件为 :1 %Na2 CO3,温度 55℃ ,时间 2h .经碱溶酸沉后的乳清液 ,采用超滤法除残留蛋白 ,通过正交实验确定的纯化条件为 :温度 2 5℃ ,pH值 6 3,膜压力 2 0psi.离子交换脱盐后 ,经真空减压浓缩得到产品
【Abstract】 Extraction effect of soybean oligosacchride in various solvents was compared using cooled defatted soybean meals as raw material.The better conditions were:1%Na 2CO 3,extraction temperature 55℃ and extraction time 2 hours.After being dissolved by alkali then being precipitated by acid,remaining protein was removed by Ultrafiltration(UF) and through orthogonal tests.The optimum condition was:25℃,pH6.3,and membrane prssure 20 psi.The product was obtained by concentrated under vacuum after desalting by ion exchange.
【关键词】 大豆低聚糖;
低温脱脂大豆粕;
浸提;
超滤;
【Key words】 soybean oligosacchride; cooled defatted soybean meals; extraction; Ultrafiltration(UF);
【Key words】 soybean oligosacchride; cooled defatted soybean meals; extraction; Ultrafiltration(UF);
- 【文献出处】 郑州工程学院学报 ,Journal of Zhengzhou Grain College , 编辑部邮箱 ,2001年02期
- 【分类号】TQ914
- 【被引频次】33
- 【下载频次】480