节点文献

毛细管柱气相色谱法测定风油精中主要成分的含量

Determination of Main Compositions in the Essential Balm by Capillary Gas Chromatography

  • 推荐 CAJ下载
  • PDF下载
  • 不支持迅雷等下载工具,请取消加速工具后下载。

【作者】 陆俭洁;

【Author】 Lu Jianjie

【机构】 中南民族学院化学系;

【摘要】 采用 GC- 90 0型气相色谱仪 ,毛细管程序升温法 ,将风油精中 10多种成分进行了有效分离 ,测定风油精中樟脑、薄荷脑、水杨酸甲酯 3种主要成分的含量 ,得出了较为理想的色谱图 ,用内标法测定樟脑的回收率为 10 6 .2 9% ,RSD为 2 .56 % ;薄荷脑的回收率为 10 2 .4 4 % ,RSD为 1.52% ;水杨酸甲脂的回收率为 98.38% ,RSD为 1.35% .

【Abstract】 The method of the capillary column with programmed temperature gas chromatography was used by the GC 900 gas chromatograph. Many kinds of compositions in the essential balm can be separated effectively by the method. The three main compositions that are camphor, menthol and methyl salicylate were quantified and satisfactory chromatogram was obtained. By the internal standard method, the recovery of determining the camphor, menthol, methyl salicylate are 106.29 %, 102.44 %, 98.38 % and RSD are 0.06 %, 2.62 % ,1.88 % respectively.

  • 【文献出处】 中南民族学院学报(自然科学版) ,Journal of South-central College For Nationalities(Natural Sciences) , 编辑部邮箱 ,2001年02期
  • 【分类号】O657.7
  • 【被引频次】4
  • 【下载频次】384
节点文献中: