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双波长薄层扫描法测定腰腿痛丸中麻黄碱含量

Determination of Ephedrine Content in Yaotuitong Pill by TLC-densitometry

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【作者】 尚立霞张玲胡庆文单卫华郭承军时延增

【Author】 SHANG Li xia, ZHANG Ling, HU Qing Wen, SHAN Wei hua, GUO Cheng jun, SHI Yan zeng (Shandong Academy of Biopharm, Jinan 250014, China)

【机构】 山东省生物药物研究院!山东济南250014

【摘要】 目的 :采用双波长薄层扫描法测定腰腿痛丸中麻黄碱的含量。方法 :样品超声处理 ,离心后取上清液 ,在 λS=5 1 5 nm,λR=6 80 nm下测定含量。结果 :方法简便、准确度高 ,精密度好。结论 :可作腰腿痛丸的质控方法

【Abstract】 Objective:This paper reported a method of quantitative analysis for ephedrine content in Yaotuitong Pill by TLC densitometry. Methods:The samples were extracted with ultrasonic treatment, were seperated by TLC after centrifugalization, then determined at λ S =515 nm, λ R =680 nm. Results:The result proved that the method was simple, rapid and accurate. Conclusion:It is suitable for the determination of ephedrine content in Yaotuitong Pill.

【关键词】 腰腿痛丸薄层扫描法麻黄麻黄碱
【Key words】 Yaotuitong PillTLC densitometryHerba EphedraeEphedrine
  • 【文献出处】 时珍国医国药 ,LiShiZhen Medicine and Materia Medica Research , 编辑部邮箱 ,2001年05期
  • 【分类号】R287
  • 【被引频次】1
  • 【下载频次】33
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