【摘要】 采用非水相毛细管电泳法分离雷公藤中雷公藤次碱 .优化条件是 :操作电压 15kV ,温度保持30 1K ,动力进样 5s ,运行介质为 2 0mmol/L醋酸铵和 3mmol/L氨水加到甲醇媒介中 .实验结果证明此方法是可行的更多还原

【Abstract】 A capillary eletrophoresis using nonaqueous buffers as background electrolytes was developed for the determination of wilforine in Tripterygium wilfordii hook f.The optimum separation conditions are as follows: voltage 15 kV, the temperature was kept at 301 K, hydrodynamic injection for 5 s, the running medium consisted of 20 mmol/L of ammonium acetate and 3 mmol /L ammonium hydroxide in methanol. The feasibility of this method was demonstrated by the determination of wilforine in Tripterygium wilfordii hook f.更多还原