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灭幼脲和吡虫啉杀虫混剂的高效液相色谱分析
Determination of Dichlorbenzuron and Imidacloprid In the Mixture by HPLC
【摘要】 采用高效液相色谱法对灭幼脲和吡虫啉杀虫混剂进行了分析。以甲醇和水为流动相 ,μBandapakphenye色谱柱为固定相 ,在 2 5 4nm下检测 ,内标法定量分析。吡虫啉、灭幼脲线性相关系数分别为 0 9984、0 9998,变异系数分别为 0 45 %、0 5 4%。
【Abstract】 A method for the determination of dichlorbenzuron and imidacloprid by HPLC on μBandapak phenye column and UV detector(254nm)was established.The mobile phase consists of methanol-water(63/37,V/V).Using internal standard method,the results showsed that the linear correlation of imidadoprid and dichlorbenzuron were 0 9984 and 0.9998,coefficient of variation were 0.45% and 0.54% respectively.
【关键词】 高效液相色谱;
吡虫啉;
灭幼脲;
内标法;
【Key words】 HPLC; dichlorbenzuron; imidacloprid; internal standard method.;
【Key words】 HPLC; dichlorbenzuron; imidacloprid; internal standard method.;
- 【文献出处】 农药 ,PESTICIDES , 编辑部邮箱 ,2000年03期
- 【分类号】TQ453
- 【被引频次】3
- 【下载频次】115