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金属间化合物提高陶瓷接头高温性能的作用

HEAT-RESISTANT Si3N4 CERAMIC JOINTS WITH INTERMETALLIC COMPOUNDS FORMED IN SITU

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【作者】 吴爱萍; 邹贵生; 任家烈; 任维佳; 李盛;

【Author】 WU Aiping, ZOU Guisheng, REN Jialie, REN Weijia, LI Sheng ( Department of Mechanical Engineering, Tsinghua University, Beijing 100084) Correspondent: WU Aiping, associate professor Tel: (010)62773859, E-mail: wuaip@mail. tsinghua. edu. cn Manuscript recei

【机构】 清华大学机械工程系!北京100084;

【摘要】 研究了连接过程中通过原位形成金属间化合物来提高 Si3N4陶瓷接头高温性能的可能性、研究了用 Ti/Ni/Ti多层中间层在 1000—1150℃t温度范围内以过渡液相连接 Si3N4陶瓷时 Ti和 Ni层厚度、连接时施加的压力以及连接温度与保温时间等因素对接头组织和强度(包括室温和高温强度)的影响规律.结果表明,在合理控制连接工艺和中间层金属厚度的条件下,可以通过原位形成金属间化合物获得室温和高温强度均较好的接头,800 ℃时接头的剪切强度可保持 88 MPa左右

【Abstract】 The possibility of the heat--resistant Si3N4 ceramic joints with intermetallic compounds formed in situ was investigated. The Si3N4 ceramics were joined with Ti/Ni/Ti multi-interlayers within 1000-1150℃. The effects of various parameters, which include the thickness of Ti and Ni foils, the pressure imposed during bonding, the bonding temperature and the holding time, on the microstructures and the strength (both at room temperature and at high temperature) of the joints were studied. The results indicated that the sound joints with higher strength both at room temperature and at elevated temperature could be acquired with intermetallic compounds formed in situ under appropriate bonding parameters. The shear strength at 800 ℃could sustain about 88 MPa.

【基金】 国家自然科学基金!项目59675056;博士学科点专项科研基金项目!9500333资助
  • 【文献出处】 金属学报 ,Acta Metallrugica Sinica , 编辑部邮箱 ,2000年11期
  • 【分类号】TG40
  • 【被引频次】8
  • 【下载频次】121
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