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薄层色谱法测定板蓝根冲剂中靛甙的含量

TLC determination of indican in granules of banlangen

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【作者】 张文英; 田桂杰; 应荣多;

【Author】 Zhang We; Tha Gedie; Ying Rongduo(Tianjin Medical University, Tianjin 300203)

【机构】 天津医科大学!天津300203;

【摘要】 采用生药中所含靛式经水解后与吲哚醌缩合生成靛玉红,然后用薄层色谱法对靛玉红进行测定的新方法,对不同厂家的板蓝根冲剂进行了质量分析,结果比较满意。加样回收率为98.46%,精密度测定RSD为3.6%。

【Abstract】 his paPer sugge8ts that Indican hydrolyrered be conden-sated with Isatin, into Indirubin, it may be used as a quality comtrolstandord for the granules of Banlangen This provides a reliable method forthe quality control of Banlangen and its preparations.Its content is determined by TLC, The meth0d showed good linearity (r =0. 9999. n = 5) in the range of 0. O8 ~ O. 24 μg/ml of Indirubin. Theaverage recovery rate was ab0ut 98. 46% with RSD < 3. 6% (n = 3).

【关键词】 板蓝根冲剂; 靛甙; 靛玉红; 薄层色谱法;
【Key words】 TLC; Granules of Banlangen; indirubin;
  • 【文献出处】 天津药学 ,TIANJIN PHARMACY , 编辑部邮箱 ,1999年02期
  • 【分类号】R284
  • 【被引频次】2
  • 【下载频次】142
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