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毛叶香茶菜醛-β-环糊精包合物的制备及分析

Preparation and analysis on inclusion of isodonal β cyclodextrin

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【作者】 王桂红; 寇娴; 张雁冰; 赵清治; 薛华珍;

【Author】 Wang Guihong, Kou Xian, Zhang Yanbing, Zhao Qingzhi, Xue Huazhen Department of Organic Chemistry, Henan Medical University, Zhengzhou 450052

【机构】 河南医科大学有机化学教研室!郑州450052;

【摘要】 的 :制备毛叶香茶菜醛 β 环糊精包合物。 方法 :采用沉淀法在水溶液中制备毛叶香茶菜醛 β 环糊精包合物 ,并用差示扫描量热法、比旋光度测定证明包合物的存在 ,用连续递变法测定了包合物的组成的摩尔比。结果 :用沉淀法可制得毛叶香茶菜醛 β 环糊精包合物 ,通过连续递变法证明了包合物的组成摩尔比为 1∶1。 结论 :本实验可得到收率较高、较纯的包合物 ,用连续递变法可确定包合物组成的摩尔比

【Abstract】 Aim: To prepare and analyze inclusion of isodinal β cyclodextrin. Methods: The inclusion compound of isodonal β cyclodextrin was prepared by the liquid phase method in aqueous solution. It was confirmed by different thermal analysis and specific rotations. The composition ratio of inclusion between isodonal and β cyclodextrin was obtained by the continuous variation method. Results: Inclusion of isodonal β cyclodextrin could be prepared by this way and its inclusion ratio was 1∶1. Conclusion: By using this method purer and higher recovery rate of inclusion can be obtained and inclusion’s composition ratio can be determined by different thermal analysis.

  • 【文献出处】 郑州大学学报(医学版) ,Journa of Henan Medical University , 编辑部邮箱 ,1999年03期
  • 【分类号】O636
  • 【被引频次】2
  • 【下载频次】77
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