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一种新型的ICP-AES用低功率微波热雾化系统

A Novel Low Microwave Powered Thermospray Nebulizer for Liquid Sample Introdution in Inductively Coupled Plasma Atomic Emission Spectrometry

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【作者】 丁兰; 金海燕; 徐蔚青; 梁枫; 曹彦波; 金钦汉;

【Author】 DING Lan, JIN Hai Yan, XU Wei Qing, LIANG Feng , CAO Yan Bo , JIN Qin Han  * (Center of Analysis and Test, Department of Chemistry , Jilin University, Changchun 130023, China)

【机构】 吉林大学分析测试中心!长春; 130023; 吉林大学分析测试中心!化学系; 长春;

【Abstract】 In this paper, a novel low microwave powered thermospray system was developed. In this system the focused microwave oven used in traditional microwave powered thermospray nebulizer was replaced with a TM 010 microwave resonant cavity, the high pressure pump was replaced with a peristaltic pump. This improvement makes the thermospray system more compact and economical. The influence of several experimental variables(concentration of acid, sample uptake rate, carrier flow rate) on the emission intensity of Mg was evaluated. Compared with the pneumatic nebulization, the detection limits for Mg of this system was improved by a factor of 4.

【关键词】 热雾化; 电感耦合等离子体发射光谱; 微波;
【Key words】 Thermospray; ICP-AES; Microwave;
【基金】 国家自然科学基金!(批准号 :29735160)资助课题
  • 【文献出处】 高等学校化学学报 ,CHEMICAL RESEARCH IN CHINESE UNIVERSITIES , 编辑部邮箱 ,1999年12期
  • 【分类号】O657
  • 【被引频次】7
  • 【下载频次】51
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