节点文献
甲基(γ-氯丙基)二氯硅烷的制备工艺研究
Study on the Preparation Technology for Methyl(γ chloropropyl)dichlorosilane
【摘要】 以氯铂酸-胺体系为催化剂的硅氢加成法合成甲基(γ-氯丙基)二氯硅烷,考察了反应温度、原料配比、催化剂用量、反应时间等因素对反应产物收率的影响,选择出最佳工艺条件,硅氢加成收率达到81%.
【Abstract】 Methyl(γ chloropropyl)dichlorosilane was prepared by using the catalyzing of platium amine for the catalyzing hydrosilation of methyldichlorosilane with 3-chloro propene.The effect of various possible facts and the reaction conditions on the results was also investigated.It was found that the catalyst has high activity under 20/10 6.The product is obtained in 81% yield.
【关键词】 硅氢加成;
甲基二氯硅烷;
烯丙基氯;
氯铂酸;
【Key words】 hydrosilation; chloropropene methyldichloro silane; choroplatinic;
【Key words】 hydrosilation; chloropropene methyldichloro silane; choroplatinic;
【基金】 江西省重点攻关项目
- 【文献出处】 江西师范大学学报(自然科学版) ,JOURNAL OF JIANGXI NORMAL UNIVERSITY (NATURAL SCIENCES EDITION) , 编辑部邮箱 ,1996年04期
- 【分类号】O627.41
- 【被引频次】8
- 【下载频次】155