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甲基(γ-氯丙基)二氯硅烷的制备工艺研究

Study on the Preparation Technology for Methyl(γ chloropropyl)dichlorosilane

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【作者】 彭以元崔国娣许群兰

【Author】 Pen Yiyuan Cui Guodi Xu Qunlan Wang Shen (Department of Chemistry,Jiangxi Normal University,Nanchang 330027)

【机构】 江西师范大学化学系

【摘要】 以氯铂酸-胺体系为催化剂的硅氢加成法合成甲基(γ-氯丙基)二氯硅烷,考察了反应温度、原料配比、催化剂用量、反应时间等因素对反应产物收率的影响,选择出最佳工艺条件,硅氢加成收率达到81%.

【Abstract】 Methyl(γ chloropropyl)dichlorosilane was prepared by using the catalyzing of platium amine for the catalyzing hydrosilation of methyldichlorosilane with 3-chloro propene.The effect of various possible facts and the reaction conditions on the results was also investigated.It was found that the catalyst has high activity under 20/10 6.The product is obtained in 81% yield.

【基金】 江西省重点攻关项目
  • 【文献出处】 江西师范大学学报(自然科学版) ,JOURNAL OF JIANGXI NORMAL UNIVERSITY (NATURAL SCIENCES EDITION) , 编辑部邮箱 ,1996年04期
  • 【分类号】O627.41
  • 【被引频次】8
  • 【下载频次】155
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