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湖泊沉积物中邻苯二甲酸酯类的GC/MS分析
Analysis of Phthalic Esters in Lake Sediments by GC/MS
【摘要】 东湖沉积物阴干后用二氯甲烷溶剂萃取,用DB-5弹性石英毛细管柱GC/MS分离鉴定,并结合m/z149质量色谱图,确证东湖沉积物中含有9种邻苯二甲酸酯类化合物,它们是邻苯二甲酸二乙酯、二异丁酯、二正丁酯、二己酯、己基辛基酯、二-(2-乙基己基)酯、二辛酯、己基癸基酯和辛基癸基酯,其特征离子及峰度见表1。
【Abstract】 Nine phthalic esters in sediments from East lake of wuhan city have been identified by GC/MS in a DB-5 silica capillary column.They are diethyl phthalate,diisobutyl phthalate,dibutyl phthalate,dihexyl phthalate,hexyloctyl phthalate,di-(2-ethylhexyl)phthalate,dioctyl phthalate,hexyldecyl phthalate,and octyldecyl phthalate.
- 【文献出处】 分析测试学报 ,JOURNAL OF INSTRUMENTAL ANALYSIS , 编辑部邮箱 ,1995年05期
- 【分类号】X132
- 【被引频次】52
- 【下载频次】234