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RP-HPLC梯度淋洗法测定一步法合成抗氧剂1010的组分
Determination of Components of Antioxide 1010 of One-step Synthesis by RP-HPLC with Gradient Elution
【摘要】 本文报道采用RP-HPLC梯度淋洗法测定一步法合成抗氧剂1010的组分,色谱分离出十一个特征吸收峰。用外标法和内标法定量对比,其各组分的回:收率为94.51~100.82%,灵敏度为0.49~3.21μg,变异系数在0.80~1.91%范围内。本法准确、灵敏,可满足科研和工业生产的定量分析要求。
【Abstract】 Eleven components in antioxide 1010 of one-step synthesis have been determined by RP-HPLC with gradient elution using external and internal standards. The recoveries, sensitivities,and variation coeffisients of this method are 94.51~100.82%, 0.49~3,21μg and 0.80~1.91%respectively.
- 【文献出处】 分析测试通报 ,Journal of Instrumental Analysis , 编辑部邮箱 ,1990年02期
- 【被引频次】1
- 【下载频次】75