In alkaline condition mesoporous Y-MCM-41 materials have been successfully synthesized using microwave heating. XRD、 FT-IR、 SEM、 TEM and N_2 adsorption-desorption experiments have been used to characterize the samples. The results show that the sample possesss a hexagonal array of uniform mesopores and the surface area about 650.4?m~2/g. X-ray fluorescence spectrum analysis (demonstrates) that 0.6% Y exists in the mesoporous structure of Y-MCM-41. The conclusion has also been confirmed by FT-IR which shows ...