In recent years, monolithic column as the stationary phase of high performance liquidchromatography (HPLC), has attracted increasing attention because of its excellent masstransfer properties and versatile surface modification compared to conventional columnspacked with particles. Redox initiator can fast occur under contact pressure and ambienttemperature condition, and shorten the initiation time. In this dissertation, redox initiator wasused to initiate the free radical polymerization to prepare the poly...