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TiO2/WO3纳米粉体的制备及其光催化性能

Study on the preparation of TiO2/WO3 and Its Photocatalytic Activity

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【作者】 刘华俊

【Author】 LIU Hua-jun(Department of Chemistry & Biology Science,Xiangfan University,Xiangfan 441053,China)

【机构】 襄樊学院化学与生物科学系 湖北襄樊441053

【摘要】 以Na2WO4和C12H25NH3.Cl作原料,通过液相沉淀法制备了WO3纳米粉体,再用钛酸胶体浸滞法制备了TiO2包覆的WO3纳米粉体,并采用透射电子显微镜、紫外-可见漫反射吸收光谱和X-射线衍射对其结构进行了表征.实验结果表明,TiO2包覆使WO3的光响应范围扩大,吸附量增大,显著提高了WO3对可溶性染料罗丹明B的光催化降解活性和光稳定性.

【Abstract】 Columnar WO3 nanoparticles have been prepared from Na2WO4 and C12H25NH3.Cl via a liquid precipitation process,and TiO2-coated WO3 nanoparticles were synthesized by solvent impregnating method with TiO2 colloid.The obtained samples were characterized by X-ray diffraction,transmission electron microscopy,the UV-vis diffuse reflectance spectrum.Moreover,the samples were employed for degradation of Rhodamine B in aqueous suspension.The results showed that TiO2 coating enhanced the photocatalytic activity and photostability of WO3 for Rhodamine B degradation.

【关键词】 光催化降解罗丹明BTiO2WO3
【Key words】 PhotocatalysisRhodamine BTiO2WO3
【基金】 湖北省教育厅科研项目(D200625003)
  • 【文献出处】 襄樊学院学报 ,Journal of Xiangfan University , 编辑部邮箱 ,2007年05期
  • 【分类号】O643
  • 【被引频次】8
  • 【下载频次】196
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