【摘要】 本文提出了一种GC-FPD测定海水中28种有机磷农药残留的新方法。采用双柱法,即选用DB-1701柱进行定性、定量分析,用HP-5柱验证。既发挥了FPD检测器灵敏、定量准确的优点,又利用了双柱法的定性功能。方法对各目标物均有良好的线性关系,回收率和RSD分别在70.2%~103.2%、8.7%~17.5%之间,适合于海洋水体中痕量有机磷农药的分析。更多还原

【Abstract】 A GC method has been developed to determine 28 kinds of OPPs in seawater simultaneously by GC-FPD.The columns were DB-1701 and HP5.The column DB-1701 used for analysis and the column HP-5 used for validate.The linear dynamic ranges were well.the recovery was from70.2 %～103.2 %,the RSD was from 8.7 %～17.5 %.The method was used for the determination of trace OPPs in sea water.更多还原