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Co-Fe普鲁士蓝类配合物纳米颗粒的微乳液法制备与表征(英文)

Synthesis and Characterization of Cobalt-iron Prussian Blue Analogue Nanoparticles by Microemulsion

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【Author】 FANG Jian1 DU Xian-Long1 LU Hui-Hong1 GUO Dan1 ZHAO Ji-Hua*,1 SHEN Wei-Guo2 (1Department of Chemistry, Lanzhou University, Lanzhou 730000) (2Department of Chemistry, East China University of Science and Technology, Shanghai 200237)

【机构】兰州大学化学化工学院；华东理工大学化学学院兰州730000；兰州730000；上海200237；

【摘要】 Highly oriented cubic, hollow cubic and spherical nanoparticles of cobalt-iron Prussian blue analogues were synthesized in poly oxyethylene tertoctylphenyl ether (TritonX-100)/n-hexanol/cyclohexane microemulsion. The effects of the water-to-surfactant molar ratio (w), the reactant concentration and the reaction temperature on the morphology of cobalt-iron Prussian blue analogues were studied. The samples were characterized by transmission electron microscopy (TEM), field emission scan electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDS), X-ray diffraction (XRD) and infrared spectroscopy (IR).更多还原

【Abstract】 Highly oriented cubic, hollow cubic and spherical nanoparticles of cobalt-iron Prussian blue analogues were synthesized in poly oxyethylene tertoctylphenyl ether (TritonX-100)/n-hexanol/cyclohexane microemulsion. The effects of the water-to-surfactant molar ratio (w), the reactant concentration and the reaction temperature on the morphology of cobalt-iron Prussian blue analogues were studied. The samples were characterized by transmission electron microscopy (TEM), field emission scan electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDS), X-ray diffraction (XRD) and infrared spectroscopy (IR).更多还原

【关键词】微乳液； TritonX-100；普鲁士蓝类配合物；纳米颗粒；
【Key words】 microemulsion； Triton X-100； Prussian blue analogues； nanoparticle；

【基金】国家自然科学基金资助项目(No.20603014,20473035)。

【文献出处】无机化学学报 ,Chinese Journal of Inorganic Chemistry , 编辑部邮箱 ,2007年05期

【分类号】O641.4
【被引频次】6
【下载频次】327

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