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溶胶-凝胶涂附电纺纳米纤维制备ZrO2纳米管
Zirconium Dioxide Nanotubes from Sol-gel Coating of Electrospun Polymer Fibers
【摘要】 <正>二氧化锆作为一种特殊的过渡金属氧化物,具有优异的耐热、耐腐蚀和可塑性,除大量应用于耐火材料外,还广泛用于制造压电元件、陶瓷电容器、气
【Abstract】 Stable zirconia sol was prepared using inorganic salt(zirconia chloride octahydrate) as the precursor and H2O2 as the catalyst. ZrO2-PBS coaxial nanofibers were fabricated using the sol-gel coating technique to filling poly butylenes succinate(PBS) fibers with zirconium dioxide by electrospun. ZrO2 nanotubes were obtained via calcining ZrO2-PBS coaxial nanofibers. The ZrO2 nanotubes were characterized by TG, SEM and TEM, respectively. The results show that ZrO2 nanotubes with a diameter of 50100 nm are obtained after calcining ZrO2-PBS coaxial nanofibers at 450 ℃.
【基金】 国家自然科学基金项目(50503001);教育部新世纪优秀人才支持计划(NCET-05-0204);北京市教委科技发展计划重点项目(KZ200510012010);北京市优秀人才培养计划(20051D0500101);北京市市属市管高等学校人才强教计划资助。
- 【文献出处】 无机化学学报 ,Chinese Journal of Inorganic Chemistry , 编辑部邮箱 ,2007年05期
- 【分类号】O614.5
- 【被引频次】13
- 【下载频次】496