【摘要】 采用高效液相色谱法建立抗癌散正丁醇部位指纹图谱。以Kromasil 100A C18色谱柱,采用乙腈和水梯度洗脱,流速为1 mL/min,柱温为40℃,检测波为203 nm。从这10批抗癌散药材的分析结果可看出,指纹图谱相似度较高,说明不同批抗癌散药材的化学组成一致性较好,质量稳定。更多还原

【Abstract】 High performance liquid chromatography(HPLC) was used to establish the fingerprint of n-butylol extraction of Kangaisan.The Kromasil 100A C18 chromatographic column with the conditions was chose as follows: velocity of flow was 1 mL/min,the column temperature was 40 ℃ and the detective wave length was 203 nm.The result showed that the ten groups Kangaisan medicinal materials had high recurrence,which indicated that the chemical elements in different origin of Kangaisan medicinal materials were similar.It was concluded that the quality of Kangaisan compound was steady.更多还原