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乳酸丁酯的合成及分析

Catalytic synthesis of butyl lactate

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【作者】 苏本玉陈震曹晓群

【Author】 SU Ben-yu1,CHEN Zhen2,CAO Xiao-qun2(1.Shandong institute of supervision and inspection on product quality,Jinan 250100,China;2.Taishan Medical College,Taian 271000,China)

【机构】 山东省产品质量监督检验研究院泰山医学院泰山医学院 山东济南250100山东泰安271000

【摘要】 目的催化合成乳酸丁酯。方法以乳酸和正丁醇为原料,用催化剂NS-2催化合成乳酸丁酯,探讨了酯化反应的最佳反应条件。结果当正丁醇、乳酸的摩尔比为1.3:1,催化剂用量占反应物料总质量的1.5%时,反应2.5小时,酯收率达到94.5(。结论该催化剂价廉易得,反应条件温和,不腐蚀设备,有推广应用价值。

【Abstract】 Objective: To synthesize Butyl Lactate with new catalyst.Methods: Butyl Lactate was synthesized from lactic acid and n-butyl alcohol.NS-2 was used as catalyst and the reaction conditions were discussed.Results: The yield of the ester reached 94.5﹪ on condition that the moleculer of the alcohol and the acid were 1.3:1 and the time of refluxing was 2.5h and the amount of catalyst was 1.5% of total mass of the reactant.Conclusion: The catalyst NS-2 is simple and applicable.

【关键词】 催化合成乳酸丁酯
【Key words】 catalysissynthesisbutyl lactate
  • 【文献出处】 泰山医学院学报 ,Journal of Taishan Medical College , 编辑部邮箱 ,2007年04期
  • 【分类号】TQ225.24
  • 【被引频次】4
  • 【下载频次】186
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